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                        <gco:CharacterString>Radiocarbon Analyses - Soil samples were analyzed at the University of Georgia Center for Applied Isotope Studies (CAIS) by Accelerator Mass Spectrometry (AMS) to determine 14C radiocarbon ages. Bulk soil samples were dried at room temperature within 6 weeks of collection in the field. Samples were then submitted to CAIS where humic acid separation and analysis was performed using the following method: root material and other organics were partially removed by sieving through 125 µm nylon mesh. The resulting soil was then treated with 1N hydrochloric acid at 80 ˚C for 1 hour to remove carbonates after which the samples were treated with a solution of 0.5M Na4P2O7 and 0.1M NaOH at room temperature over 24 hours for humic acid extraction. Samples were then precipitated and centrifuged with concentrated hydrochloric acid. Finally, samples were rinsed with Milli_Q water and dried at 105 ˚C overnight. Dried samples were combusted at 900 ˚C in an evacuated sealed quartz ampoule in the presence of CuO. Graphite 14C/13C ratios were measured with a 0.5 MeV accelerator mass spectrometer with isotope ratios compared to Oxalic Acid II (NBS SRM 4990C). Ratios of 13C/12C were measured separately using a stable isotope ratio mass spectrometer and are reported as δ13C relative to Pee Dee Belemnite (PDB). Reported uncalibrated ages (AgeInterpreted) are given in radiocarbon years before 1950 using a 14C half-life of 5568 years.</gco:CharacterString>
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